Acetyl chloride → HCID 21465661, compound

HRID 1940024Notes

Reaction equation

HRID 1940024 reaction equation
[C:1]([O:4][C:5]1[C:6](=[O:13])[CH:7]([CH3:12])[O:8][C:9]=1[CH2:10]C)(=[O:3])[CH3:2].[C:14](Cl)(=O)C>>[C:1]([O:4][C:5]1[C:6](=[O:13])[CH:7]([CH2:12][CH3:14])[O:8][C:9]=1[CH3:10])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 6367Acetyl chlorideHCID 21465667HCID 21465667, compound

Product 1

HCID 21465661HCID 21465661, compound

Procedure

A mixture (1.08 g) of 4-acetoxy-2-ethyl-5-methyl-3(2H)-furanone (major) and 4-acetoxy-5-ethyl-2-methyl-3(2H)-furanone (minor) was obtained by the same method as in Preparation Example 2 except that 0.54 ml of acetyl chloride was used rather than 0.95 ml of pivaloyl chloride.

Sources & evidence

ORD record
ord-2d490a7584554ca68cd4ba5cb6498e05
Source dataset
uspto-grants-1997_12
Patent number
US05698585

Reaction notes

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