Sodium Hydroxide → HCID 22114233, compound

HRID 1940160Notes

Reaction equation

HRID 1940160 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:12]=[CH:13][C:14]=1[O:15][CH3:16])[O:5][CH2:6][C:7]([O:9]CC)=[O:8].[OH-].[Na+]>C1COCC1.CO>[Cl:1][C:2]1[CH:3]=[C:4]([CH:12]=[CH:13][C:14]=1[O:15][CH3:16])[O:5][CH2:6][C:7]([OH:9])=[O:8]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 22114273HCID 22114273, compound

Product 1

HCID 22114233HCID 22114233, compound

Reagents, catalysts & solvents 1

HCID 21899815MeOH tetrahydrofuranSolvent

Procedure

The above ethyl 3-chloro-4-methoxyphenoxyacetate (700 mg) was hydrolysed with 1M aq. NaOH in THF-MeOH (30 mL, 2:1) to provide the title compound as a white powder.

Sources & evidence

ORD record
ord-a9bc85b37a1f408b945bb244cf1cf38d
Source dataset
uspto-grants-1997_12
Patent number
US05698584

Reaction notes

Loading…