HuagongsheHuagongshe Chemistry Print Report · For research reference only
Mesitylene → Mesitylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Mesitylene | HCID 7947 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21466679 | HCID 21466679 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Water | HCID 962 | — |
| Product | Mesitylacetic acid | HCID 78123 | 85% |
Reaction Steps
8.0 g (0.06 tool) and 5.4 g (0.0198 mol) of n-butyl phenylsulfonyloxyacetate are reacted in 60 ml of mesitylene by the method of Example 7, and the reaction mixture is hydrolyzed with 5 g of NaOH in 15 ml of water and 50 ml of methanol to give the acid. 3.0 g (85% of theory) of mesitylacetic acid are isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698735 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-48acdc19c90045439dc3fecdc303f4a9 |
| Source note | uspto-grants-1997_12 |