HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cumylamine → N-(1-Methyl-1-phenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cumylamine | HCID 68509 | — |
| Reactant | S-2pyridyl 3-cyanoandrosta-3,5-diene-17beta-thiocarboxylate | HCID 15380265 | — |
| Product | N-(1-Methyl-1-phenylethyl)-3-cyanoandrosta-3,5-diene-17beta-carboxamide | HCID 15380257 | 75% |
Reaction Steps
A procedure similar to that described in Example 3(b) was repeated, except that S-2-pyridyl 3-cyanoandrosta-3,5-diene-17β-thiocarboxylate [prepared as described in Example 3(a)] and 1-methyl-1-phenylethylamine were used as starting materials, in relative proportions similar to those used in that Example, to give the title compound in a yield of 75%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698720 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-87d4ccde2da24c87a374f6e350f8b94f |
| Source note | uspto-grants-1997_12 |