HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butylamine → 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butylamine | HCID 6385 | — |
| Reactant | 3-Cyanoandrosta-3,5-diene-17beta-carboxylic acid | HCID 15380254 | — |
| Product | 3-Cyano-N-(1,1-dimethylethyl)androsta-3,5-diene-17-beta-carboxamide | HCID 67646951 | 81% |
Reaction Steps
Following a procedure similar to that described in Preparation 16a, but using 3-cyanoandrosta-3,5-diene-17β-carboxylic acid [prepared as described in Example 1(b)] and t-butylamine as starting materials, in relative proportions similar to those used in that Preparation, the title compound was obtained in a yield of 81%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05698720 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-5d79ba24b1ba4d0c9bf8d6aa3df98ed1 |
| Source note | uspto-grants-1997_12 |