HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → N-(2-mercaptoethyl)-N'-(2-hydroxyethyl)succinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 4-Oxo-4-[(2-sulfanylethyl)amino]butanoic acid | HCID 22450828 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N-(2-mercaptoethyl)-N'-(2-hydroxyethyl)succinamide | HCID 15293891 | — |
Reaction Steps
A solution of 4.4 g (23 mmol) of methyl ester of N-(2-mercaptoethyl)succinamic acid obtained in Example 1a) in 20 cm3 of methanol, and 1.68 g (27 mmol) of ethanolamine was stirred for 5 hours at 60° C. under argon atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700454 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-26daed83f0234386b096de864a887ea0 |
| Source note | uspto-grants-1997_12 |