HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21462233, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 21462225 | HCID 21462225 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21462233 | HCID 21462233 | — |
Reaction Steps
4-Hydroxymethyl-8-methylthio-2,2,6,6-tetramethylbenzo[1,2-d:4,5-d']bis(1,3)dioxole is dissolved in pyridine. The solution is chilled and triphenylphosphine followed by carbontetrabromide are added. the reaction is stirred for an appropriate time. Methanol is added and the product is isolated by a suitable method.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700448 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-fcd6e00060dd472ab132f83cfe5a0dbe |
| Source note | uspto-grants-1997_12 |