HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178522205, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | bromine AcOH | HCID 87433071 | — |
| Reactant | HCID 178522206 | HCID 178522206 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178522205 | HCID 178522205 | 67% |
Reaction Steps
To a solution of the title compound from Example 263 (0.34 grams) and glacial acetic acid (10 mL) was added a 0.7M bromine-acetic acid solution (4 mL) at 25° C. under N2. After 10 minutes, water was added and the resulting solid was filtered and washed with water several times and dried to give the title compound (Yield 0.31 grams, 67%, MH+ 527).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700806 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-a7a574b6bc9142a7ba16774ab0a440ac |
| Source note | uspto-grants-1997_12 |