HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → HCID 10825977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | HCID 10589187 | HCID 10589187 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 10825977 | HCID 10825977 | — |
Reaction Steps
600 mg of N-diaminomethylene-2-methyl-4-methoxy-5-methylsulfonylbenzamide (obtainable according to Ex. 2) are boiled for 3 hours in 80 ml of pyridine together with 1 g of pyridine hydrochloride. The mixture is cooled and evaporated, and the residue is worked up in the customary manner to give N-diaminomethylene-2-methyl-4-hydroxy-5-methylsulfonylbenzamide, m.p. >260°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05700839 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-bdbdcd1415cb46d5bbb76644f12afc20 |
| Source note | uspto-grants-1997_12 |