Formaldehyde → HCID 21463222, compound

HRID 1940961Notes

Reaction equation

HRID 1940961 reaction equation
Cl.[CH3:2][C:3]1[CH:4]=[C:5]([CH:31]=[C:32]([CH3:34])[CH:33]=1)[CH2:6][NH:7][CH:8]1[C:17]2[N:12]([C:13](=[O:30])[C:14]3[CH:27]=[C:26]([CH3:28])[C:25]([CH3:29])=[CH:24][C:15]=3[C:16]=2[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)[CH2:11][CH2:10][CH2:9]1.[CH2:35]=O.[BH4-].[Na+]>>[CH3:28][C:26]1[C:25]([CH3:29])=[CH:24][C:15]2[C:16]([C:18]3[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=3)=[C:17]3[N:12]([C:13](=[O:30])[C:14]=2[CH:27]=1)[CH2:11][CH2:10][CH2:9][CH:8]3[N:7]([CH2:6][C:5]1[CH:4]=[C:3]([CH3:2])[CH:33]=[C:32]([CH3:34])[CH:31]=1)[CH3:35]

Participants

4

Reactant 3

HCID 712FormaldehydeHCID 4311764Sodium borohydrideHCID 21463326HCID 21463326, compound

Product 1

HCID 21463222HCID 21463222, compound

Procedure

The compound obtained in Example 233 and formalin were reacted and treated with sodium borohydride in the same manner as in Example 233 to yield the title compound as colorless crystals.

Sources & evidence

ORD record
ord-aefb2d73edd446f8b15352b64da8b913
Source dataset
uspto-grants-1997_12
Patent number
US05700810

Reaction notes

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