HuagongsheHuagongshe Chemistry Print Report · For research reference only
12-Bromododecyl prop-2-enoate → HCID 21459494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 12-Bromododecyl prop-2-enoate | HCID 13841397 | — |
| Reactant | 6-Bromohexyl prop-2-enoate | HCID 15153819 | — |
| Reactant | 2,3-Difluoro-4'-[6-(acryloyloxy)hexyloxy]biphenyl | HCID 21459498 | — |
| Product | HCID 21459494 | HCID 21459494 | 24.1% |
Reaction Steps
The same procedure as in the synthesis (b) of Example 2 was repeated except that 6.7 g of 12-bromododecyl acrylate were used instead of 5.0 g of 6-bromohexyl acrylate to give 2.1 g (Y., 24.1%) of 2,3-difluoro-4'-[12-(acryloyloxy)dodecyloxy]biphenyl. m.p.; 59.7°-60.7° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702642 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-3ca8e802c8a24540b6578d3271d6e80c |
| Source note | uspto-grants-1997_12 |