HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-1-hexanol → 8-Bromooctyl prop-2-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-1-hexanol | HCID 77970 | — |
| Reactant | 1-Octanol, 8-bromo- | HCID 162607 | — |
| Reactant | 2,3-Difluoro-4'-[6-(acryloyloxy)hexyloxy]biphenyl | HCID 21459498 | — |
| Product | 8-Bromooctyl prop-2-enoate | HCID 13841395 | 78% |
Reaction Steps
The same procedure as in the synthesis (a) of Example 2 was repeated except that 34.7 g of 8-bromo-1-octanol were used instead of 30 g of 6-bromo-1-hexanol to give 34.1 g (Y., 78%) of 8-acryloyloxy-1-bromooctane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702642 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-528b809ea1af49fe8275514e820f353d |
| Source note | uspto-grants-1997_12 |