Cesium carbonate → HCID 22071086, compound

HRID 1941080Notes

Reaction equation

HRID 1941080 reaction equation
[OH:1][C:2]1[CH:15]=[CH:14][C:13]2[C:12]([C:16]([OH:18])=[O:17])=[C:11]3[C:6]([CH:7]=[C:8]4[CH:22]=[CH:21][CH:20]=[CH:19][C:9]4=[CH:10]3)=[N:5][C:4]=2[CH:3]=1.C(=O)([O-])[O-].[Cs+].[Cs+].Br.[CH2:30]([N:32]([CH2:35][CH2:36]Br)[CH2:33][CH3:34])[CH3:31]>>[CH2:30]([N:32]([CH2:35][CH2:36][O:1][C:2]1[CH:15]=[CH:14][C:13]2[C:12]([C:16]([O:18][CH2:31][CH2:30][N:32]([CH2:35][CH3:36])[CH2:33][CH3:34])=[O:17])=[C:11]3[C:6]([CH:7]=[C:8]4[CH:22]=[CH:21][CH:20]=[CH:19][C:9]4=[CH:10]3)=[N:5][C:4]=2[CH:3]=1)[CH2:33][CH3:34])[CH3:31]

Participants

4

Reactant 3

HCID 10796Cesium carbonateHCID 706072-Bromoethyldiethylammonium bromideHCID 136119075HCID 136119075, compound

Product 1

HCID 22071086HCID 22071086, compound

Procedure

treating 3-hydroxy-benz[b]acridine-12-carboxylic acid with cesium carbonate and diethylaminoethyl bromide hydrobromide to produce N,N-diethylaminoethyl 3-(N,N-diethylamino)ethoxy-benz[b]acridine-12-carboxylate;

Sources & evidence

ORD record
ord-ca85c7f270f04439aefd575b9c3708ea
Source dataset
uspto-grants-1997_12
Patent number
US05702887

Reaction notes

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