HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → Phthalocyanine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 136396736 | HCID 136396736 | — |
| Product | Phthalocyanine | HCID 86280045 | — |
Reaction Steps
Chloroaluminium phthalocyanine tetrasulphonate (100 mg, 1.12×10"4 mol) is dried overnight at 100° C. Phosphorus oxychloride (410 μl, 4.48×10-3 mol) is added and the mixture is incubated at ambient temperature under exclusion of moisture. After 24 hours at this temperature, unreacted phosphorus oxychloride is removed by bulb-bulb distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05702952 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-b1c96b19bb934ff9b8d6ba32d0bef848 |
| Source note | uspto-grants-1997_12 |