Sodium Hydroxide → HCID 86751765, compound

HRID 1941092Notes

Reaction equation

HRID 1941092 reaction equation
[CH3:1][O:2][C:3]([NH:5][N:6]=[CH:7][C:8]1[CH:13]=[CH:12][C:11]([NH:14][C:15](=[O:23])[NH:16][CH2:17][C:18]([O:20]CC)=[O:19])=[CH:10][CH:9]=1)=[O:4].[OH-].[Na+:25]>C(O)C>[CH3:1][O:2][C:3]([NH:5][N:6]=[CH:7][C:8]1[CH:9]=[CH:10][C:11]([NH:14][C:15](=[O:23])[NH:16][CH2:17][C:18]([O-:20])=[O:19])=[CH:12][CH:13]=1)=[O:4].[Na+:25]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 86751764HCID 86751764, compound

Product 1

HCID 86751765HCID 86751765, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

5.15 g (15.98 mmol) of ethyl (3-(4-(methoxycarbonylaminoiminomethyl)phenyl)ureido)acetate are dissolved in 200 ml of ethanol and treated with 7.99 ml (15.98 mmol) of a 2N NaOH and the mixture is stirred at room temperature for 24 h. It is then concentrated in vacuo and the residue is freeze-dried.

Workup

  1. concentrationIt is then concentrated in vacuo
  2. customthe residue is freeze-dried

Sources & evidence

ORD record
ord-eba9c6a9adce430d8b6cfcc1cddd90b8
Source dataset
uspto-grants-1997_12
Patent number
US05703050

Reaction notes

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