Sodium Hydroxide → HCID 86751767, compound

HRID 1941094Notes

Reaction equation

HRID 1941094 reaction equation
[CH2:1]([O:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[CH:19]=[CH:18][C:17]([NH:20][C:21](=[O:29])[NH:22][CH2:23][C:24]([O:26]CC)=[O:25])=[CH:16][CH:15]=1)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH-].[Na+:31]>C(O)C>[CH2:1]([O:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[CH:15]=[CH:16][C:17]([NH:20][C:21](=[O:29])[NH:22][CH2:23][C:24]([O-:26])=[O:25])=[CH:18][CH:19]=1)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Na+:31]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 86751766HCID 86751766, compound

Product 1

HCID 86751767HCID 86751767, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

0.74 g (1.86 mmol) of ethyl (3-(4-(benzyloxycarbonylaminoiminomethyl)phenyl)ureido)acetate in 100 ml of ethanol is treated with 1.86 ml of 1N NaOH and the mixture is stirred at room temperature for 6 h. The solvent is removed in vacuo and the residue is freeze-dried.

Workup

  1. customThe solvent is removed in vacuo
  2. customthe residue is freeze-dried

Sources & evidence

ORD record
ord-45ba783761f343b7b443f51195d47cca
Source dataset
uspto-grants-1997_12
Patent number
US05703050

Reaction notes

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