HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54097936, compound → HCID 54358548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54097936 | HCID 54097936 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54358548 | HCID 54358548 | — |
Reaction Steps
Using the procedure described in J. Chem. Soc., 1956, 4330, (3β,5α,11β,12α,25R)-23-bromo-12-(trichloroacetoxy)-spirostan-3,11-diol was reduced with zinc and acetic acid to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703052 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-2490f95c921f4c69ae8bdeaa72ffd4c7 |
| Source note | uspto-grants-1997_12 |