HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Ketotigogenin → HCID 22872546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Ketotigogenin | HCID 73682 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22872546 | HCID 22872546 | — |
Reaction Steps
(3β,5α,25R)spirostan-3-ol-11-one (Aldrich Chemical Company, Milwaukee, Wis. or Steraloids Inc., Wilton, N.H., or see preparation G13) was converted into the title compound via reduction with lithium aluminum hydride in THF at room temperature according to the procedure described in J. Am. Chem. Soc., 1951, 73, 1777.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703052 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-4ce242ae3d4d4be7963ecbc8893279be |
| Source note | uspto-grants-1997_12 |