HuagongsheHuagongshe Chemistry Print Report · For research reference only
82182-52-3 → HCID 22872544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 82182-52-3 | HCID 255300 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22872544 | HCID 22872544 | — |
Reaction Steps
(3β,5α,12β,25R)-3,12-di(acetoxy)spirostan-11-one (purchased from Steraloids, Inc., or see preparation G13) was converted into the title compound via reduction with lithium aluminum hydride in THF at room temperature according to the procedure described in J. Am. Chem. Soc., 1951, 73, 1777.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703052 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-f8f2847e901144f48d8b8d7242107804 |
| Source note | uspto-grants-1997_12 |