HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15788050, compound → HCID 70344240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15788050 | HCID 15788050 | — |
| Reactant | HCID 21461386 | HCID 21461386 | — |
| Product | HCID 70344240 | HCID 70344240 | 89% |
Reaction Steps
4-Methylene-9-ethyl-9-methyl-3,5,8, 10-tetraoxabicyclo [5.3.0]decane was prepared in a similar way to 4-methylene-9,9-dimethyl-3,5,8, 10-tetraoxabicyclo [5.3.0]decane starting from 142.3 mmol (40 g) of 4-bromomethyl-9-ethyl-9-methyl-3,5,8,10-tetraoxabicyclo [5.3.0]decane, fractional distillation giving 23 g (89% yield) from 53° to 56° C. (0.2 mbar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703249 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-9e053c4c40484f13ac887ffadbb97367 |
| Source note | uspto-grants-1997_12 |