HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15788050, compound → HCID 21461381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15788050 | HCID 15788050 | — |
| Reactant | HCID 21461384 | HCID 21461384 | — |
| Product | HCID 21461381 | HCID 21461381 | 43.2% |
Reaction Steps
4-Methylene-9-methyl-9-vinyl-3,5,8,10-tetraoxabicyclo[5.3.0]decane was prepared in a similar way to 4-methylene-9,9-dimethyl-3,5,8,10-tetraoxabicyclo[5.3.0]decane starting from 115.7 mmol (35 g) of 4-bromomethyl-9-methyl-9-vinyl-3,5,8, 10-tetraoxabicyclo[5.3.0]decane, fractional distillation giving 10 g (43.2% yield) at 62° C. (0.1 mbar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703249 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-86ed9212d2d34ae6884c1e80c3aaf896 |
| Source note | uspto-grants-1997_12 |