HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 86751812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | 5-(4-Hydroxybenzyl)-3-triphenylmethylthiazolidine-2,4-dione | HCID 2818126 | — |
| Reactant | HCID 53876084 | HCID 53876084 | — |
| Product | HCID 86751812 | HCID 86751812 | 81.4% |
Reaction Steps
Following a procedure similar to that described in Example 1(a), but using 1.02 g of 2-[1-(2-isopropoxy-5-pyridyl)ethylideneaminooxy]ethanol (prepared as described in Preparation 32), 2.00 g of 5-(4-hydroxybenzyl)-3-tritylthiazolidine-2,4-dione, 1.24 g of triphenylphosphine and 784 mg of diethyl azodicarboxylate, 2.39 g of the title compound were obtained as a foam-like solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703096 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-1a654193619c4aa387a6215c2ef0b3a1 |
| Source note | uspto-grants-1997_12 |