HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Hydroxyacetophenone → HCID 86751828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Hydroxyacetophenone | HCID 8487 | — |
| Reactant | 5-(4-[2-Aminooxyethoxy)benzyl]thiazolidine-2,4-dione hydrochloride | HCID 21833965 | — |
| Product | HCID 86751828 | HCID 86751828 | 84.2% |
Reaction Steps
Following a procedure similar to that described in Example 40(f), but using 0.33 g of 3'-hydroxyacetophenone and 0.70 g of 5-[4-(2-aminooxyethoxy)benzyl]-thiazolidine-2,4-dione hydrochloride [prepared as described in Example 40(e)], 0.74 g of the title compound, melting at 133°-135° C., was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05703096 |
| Source dataset | uspto-grants-1997_12 |
| ORD ID | ord-20539e8272b540f98b8b700bb00c8217 |
| Source note | uspto-grants-1997_12 |