HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-2-picolinic acid → HCID 53241001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-2-picolinic acid | HCID 2762872 | — |
| Reactant | HCID 58304200 | HCID 58304200 | — |
| Product | HCID 53241001 | HCID 53241001 | — |
Reaction Steps
The condensation of (R)-4-(5-amino-2-chloro-phenyl)-5,5-difluoro-4-methyl-5,6-dihydro-4H-[1,3]oxazin-2-ylamine (intermediate XI-3) and 5-chloro-pyridine-2-carboxylic acid following procedure I yielded the title compound as an off-white solid. MS (ISP): m/z=415.2 [M+H]+, 417.1 [M+2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389513B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-a631febb319b4759b8a495d729e85ce8 |
| Source note | uspto-grants-2013_03 |