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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1942039Generated: October 30, 2026

Hydrochloric Acid → HCID 67457566, compound

https://huagongshe.com/reaction/1942039

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 59603644HCID 59603644—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 67457566HCID 67457566—

Reaction Steps

5 ml of a 4 N solution of hydrogen chloride in dioxane are added to 200 mg (0.5 mmol) of the compound from Example 90 and the mixture is stirred at RT for 1 h. The solid is then filtered off, washed in each case once with dioxane and tert-butyl methyl ether and dried under a high vacuum.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08389520B2
Source datasetuspto-grants-2013_03
ORD IDord-0ef0e9deeb6a4398b00a8e9c331df32e
Source noteuspto-grants-2013_03