HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Cyclohexanediol → HCID 52917036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Cyclohexanediol | HCID 11162 | — |
| Reactant | 2-Methanesulfonyl-5-phenylethynyl-pyrimidine | HCID 57516758 | — |
| Product | HCID 52917036 | HCID 52917036 | — |
Reaction Steps
The title compound, yellow solid, MS: m/e=295.3 (M+H+), can be prepared in accordance with the general method of example 1, step 3 from 2-methanesulfonyl-5-phenylethynyl-pyrimidine (example 1, step 2) and cyclohexane-1,4-diol by using Cs2CO3 as base and dioxane as solvent for 16 hours at 100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389536B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-cde4bb7371e14a29acf90aea26ba73bc |
| Source note | uspto-grants-2013_03 |