HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amine → Naphthalene-2-carboxylic acid {4-[ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amino]-butyl}-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amine | HCID 66937583 | — |
| Reactant | Naphthalene-2-carboxylic acid (4-oxo-butyl)-amide | HCID 86651298 | — |
| Product | Naphthalene-2-carboxylic acid {4-[ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amino]-butyl}-amide | HCID 66937553 | 22% |
Reaction Steps
Compound 4 is prepared from 2E and 4C as described for 1. The salt of oxalic acid is crystallized from ethanol/diethylether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389555B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-e375467b8a6a48a998e711ce300fa4b5 |
| Source note | uspto-grants-2013_03 |