HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amine → Naphthalene-2-carboxylic acid {2-[ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amino]-ethyl}-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amine | HCID 18705889 | — |
| Reactant | Naphthalene-2-carboxylic acid (2-oxo-ethyl)-amide | HCID 86651307 | — |
| Product | Naphthalene-2-carboxylic acid {2-[ethyl-(4,5,6,7-tetrahydro-benzothiazol-6-yl)-amino]-ethyl}-amide | HCID 66937429 | 34% |
Reaction Steps
Compound 32 is prepared from 32B and 1C as described for 1. The salt of oxalic acid is crystallized from ethanol/diethylether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08389555B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-bf2704b81fba4cb284d863ce3ad89390 |
| Source note | uspto-grants-2013_03 |