HCID 563992, compound → HCID 59591536, compound

Participants

Reaction Steps

2.0 g of 10% Pd/C is added, at ambient temperature, to a solution of the protected phenol 3 (23.74 g, 0.07 mol) in 320 mL of AcOEt. The reaction medium is stirred overnight under an atmosphere of H2 then it is filtered on Celite®, washed with AcOEt. The filtrate is then concentrated under vacuum in order to produce the expected product 4 (17.02 g, 0.07 mol, 99%) in the form of a colourless oil. The crude product is used in the following stage without other purification.

Provenance & Evidence