HRID1942875

反应详情

EQUATION

反应方程式

HRID 1942875 反应方程式

PROCEDURE

实验过程

This compound was prepared from (4-chloro-6-methoxy-[1,3,5]triazin-2-yl)-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-amine and 4-chloro-N-methylaniline in analogy to example 1c. It was purified by column chromatography on Si—NH2 gel (Isolute) using ethyl acetate as eluent to give the title compound as a colorless solid in 14% yield.

WORKUP

后处理

  1. customIt was purified by column chromatography on Si—NH2 gel (Isolute)