2,4-Dichloro-6-isopropoxy-1,3,5-triazine → HCID 86640785, compound

HRID 1942887Notes

Reaction equation

HRID 1942887 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([NH2:15])[CH:6]=[CH:7][C:8]=1[N:9]1[CH:13]=[C:12]([CH3:14])[N:11]=[CH:10]1.[Cl:16][C:17]1[N:22]=[C:21](Cl)[N:20]=[C:19]([O:24][CH:25]([CH3:27])[CH3:26])[N:18]=1>>[Cl:16][C:17]1[N:18]=[C:19]([O:24][CH:25]([CH3:27])[CH3:26])[N:20]=[C:21]([NH:15][C:5]2[CH:6]=[CH:7][C:8]([N:9]3[CH:13]=[C:12]([CH3:14])[N:11]=[CH:10]3)=[C:3]([O:2][CH3:1])[CH:4]=2)[N:22]=1

Participants

3

Reactant 2

HCID 231542,4-Dichloro-6-isopropoxy-1,3,5-triazineHCID 454801813-methoxy-4-(4-methyl-1H-imidazol-1-yl)aniline

Product 1

HCID 86640785HCID 86640785, compoundYield 41%

Procedure

The title compound was prepared from 3-methoxy-4-(4-methyl-imidazol-1-yl)-phenylamine and 2,4-dichloro-6-isopropoxy-[1,3,5]triazine (Synth. Commun. 24, 2153 (1994)) in analogy to example 2a. The compound crystallized from methanol as a slightly brownish solid in 41% yield.

Workup

  1. customThe compound crystallized from methanol as a slightly brownish solid in 41% yield

Sources & evidence

ORD record
ord-6af5314f95d64c3bac3ef3dc1ae854a0
Source dataset
uspto-grants-2013_03
Patent number
US08389717B2

Reaction notes

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