反应详情

温度

25 °C

To a solution of 3-sulfinylamino-benzoyl chloride (0.033 g, 0.165 mmol) (Example 1.1) in dry deuterochloroform (0.5 ml) was added under stirring at 25° C., a solution of 2-ethyl-6-methyl-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)-phenylamine (0.050 g, 0.165 mmol) (prepared according to EP 1,006,102) in deuterochloroform (0.5 ml). After stirring for 60 hours at 25° C., a sample of the reaction mixture was submitted to 1H-NMR spectroscopy. The desired compound was detected in the reaction mixture together with unreacted starting materials. Integration of the signals showed a conversion of 40%. 1H-NMR (CDCl3, 400 MHz): 8.35 (s, 1H), 8.07 (d, 1H), 7.95 (d, 1H) 7.58 (t, 1H), 7.49 (s, 1H), 7.37 (s, 2H), 2.70 (q, 2H), 2.31 (s, 3H), 1.22 (t, 3H) ppm.

1. stirringAfter stirring for 60 hours at 25° C.