HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid dihydrate → HCID 11620876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid dihydrate | HCID 61373 | — |
| Reactant | HCID 11554272 | HCID 11554272 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 11620876 | HCID 11620876 | 74.2% |
Reaction Steps
HO2CCO2H.2H2O (40 mg, 0.32 mmol) is added to a solution of 1-(3,4-dichlorophenyl)-4,5,6,7-tetrahydro-4-(2-(4-phenylpiperidin-1-yl)ethyl)-1H-indazole (140 mg, 0.31 mmol) in 4 mL of acetone, giving 1-(3,4-dichlorophenyl)-4,5,6,7-tetrahydro-4-(2-(4-phenylpiperidin-1-yl)ethyl)-1H-indazole oxalate (125 mg, 0.23 mmol, 74%, white solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394797B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-651548a95d4548caa0cfd04bd59f7b2b |
| Source note | uspto-grants-2013_03 |