3-Hydroxy-3-phenyl-1-butyne → HCID 46891995, compound

HRID 1944032Notes

Reaction equation

HRID 1944032 reaction equation
[N:1]([CH:4]1[CH2:23][N:8]2[C:9]3[C:14]([C:15]([CH2:16][C:17]([O:19]CCC)=[O:18])=[C:7]2[CH2:6][CH2:5]1)=[CH:13][CH:12]=[CH:11][CH:10]=3)=[N+:2]=[N-:3].[C:24]1([C:30]([OH:34])([C:32]#[CH:33])[CH3:31])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1>>[OH:34][C:30]([C:32]1[N:3]=[N:2][N:1]([CH:4]2[CH2:23][N:8]3[C:9]4[C:14]([C:15]([CH2:16][C:17]([OH:19])=[O:18])=[C:7]3[CH2:6][CH2:5]2)=[CH:13][CH:12]=[CH:11][CH:10]=4)[CH:33]=1)([C:24]1[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1)[CH3:31]

Participants

3

Reactant 2

HCID 920983-Hydroxy-3-phenyl-1-butyneHCID 59487226Propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate

Product 1

HCID 46891995HCID 46891995, compound

Procedure

The title compound was prepared using procedures described in EXAMPLE 1 from propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate and 2-phenylbut-3-yn-2-ol. MS (+ESI) m/z: 417.1.

Sources & evidence

ORD record
ord-a3b054539ff24241a2f1666f2622bd58
Source dataset
uspto-grants-2013_03
Patent number
US08394819B2

Reaction notes

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