1-Ethynyl-4-fluorobenzene → HCID 46892657, compound

HRID 1944039Notes

Reaction equation

HRID 1944039 reaction equation
[N:1]([CH:4]1[CH2:23][N:8]2[C:9]3[C:14]([C:15]([CH2:16][C:17]([O:19]CCC)=[O:18])=[C:7]2[CH2:6][CH2:5]1)=[CH:13][CH:12]=[CH:11][CH:10]=3)=[N+:2]=[N-:3].[C:24]([C:26]1[CH:31]=[CH:30][C:29]([F:32])=[CH:28][CH:27]=1)#[CH:25]>>[F:32][C:29]1[CH:30]=[CH:31][C:26]([C:24]2[N:1]([CH:4]3[CH2:23][N:8]4[C:9]5[C:14]([C:15]([CH2:16][C:17]([OH:19])=[O:18])=[C:7]4[CH2:6][CH2:5]3)=[CH:13][CH:12]=[CH:11][CH:10]=5)[N:2]=[N:3][CH:25]=2)=[CH:27][CH:28]=1

Participants

3

Reactant 2

HCID 5226271-Ethynyl-4-fluorobenzeneHCID 59487226Propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate

Product 1

HCID 46892657HCID 46892657, compound

Procedure

The title compound was prepared using procedures described in EXAMPLE 3 from propyl (7-azido-6,7,8,9-tetrahydropyrido[1,2-a]indol-10-yl)acetate and 1-ethynyl-4-fluorobenzene. MS (+ESI) m/z: 391.1.

Sources & evidence

ORD record
ord-8df48cdb0ae94745954ff64f71dd85b1
Source dataset
uspto-grants-2013_03
Patent number
US08394819B2

Reaction notes

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