Triethylamine → HCID 44180517, compound

Participants

Reaction Steps

A mixture of the product of example 95 (30 mg), triethylamine (10.2 μl) and methoxyacetyl chloride (6.7 μl) was stirred at room temperature for 3 h. The reaction mixture was diluted with dichloromethane and washed with water. The organic layer was dried (MgSO4), filtered and concentrated in vacuo. The residue was purified by preparative HPLC (0→90% acetonitrile; system 1).

Provenance & Evidence