Triethylamine → HCID 66925669, compound

Participants

Reaction Steps

To a solution of 2-(3-fluoro-4,5-dimethoxy-phenyl)-ethylamine (576 mg) and triethylamine (0.8 ml) in dichloromethane (20 ml) was added dropwise at 0° C. ethylchloroformate (300 μl). The mixture was stirred for 1 h, poured into ice water, neutralized with NaHCO3 and extracted with dichloromethane. The organic layers were separated, dried (MgSO4), filtered and concentrated in vacuo. The residue was passed through a short silica column (heptane/ethyl acetate as eluent).

Provenance & Evidence