HCID 67043922, compound → HCID 86652198, compound

Participants

Reaction Steps

A mixture of 3-hydroxymethylpyridine-2-sulfonic acid methylphenylamide (0.25 g), chloroform (20 mL) and manganese (IV) oxide (3.9 g) was stirred at room temperature for 2 hours. The mixture was treated with additional manganese (IV) oxide (1.6 g) and stirred at room temperature for a further 2 hours. The mixture was filtered through hyflo and the filtrate was concentrated under reduced pressure to afford the title compound (0.10 g).

Provenance & Evidence