HRID1944727

反应详情

EQUATION

反应方程式

HRID 1944727 的结构方程式

PROCEDURE

实验过程

4-(Trifluoromethyl)benzene-1-sulfonyl chloride (1 gm) was coupled to benzylamine using conditions analogous to those used to prepare intermediate 1. Purification by chromatography yielded N-benzyl-4-(trifluoromethyl)benzenesulfonamide (770 mg). Rf=0.38 by TLC eluting with 30% ethyl acetate in heptane. MS MH+ 316.2

WORKUP

后处理

  1. customPurification by chromatography