HuagongsheHuagongshe Chemistry Print Report · For research reference only
(R)-N-[5-[2-Azido-1-[(tert-butyldimethylsilyl)oxy]ethyl]-2-(benzyloxy)phenyl]formamide → N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (R)-N-[5-[2-Azido-1-[(tert-butyldimethylsilyl)oxy]ethyl]-2-(benzyloxy)phenyl]formamide | HCID 58505165 | — |
| Reactant | (R)-5-(2-Amino-1-((tert-butyldimethylsilyl)oxy)ethyl)-8-hydroxyquinolin-2(1H)-one | HCID 59023604 | — |
| Product | N-{5-[(R)-2-amino-1-(tert-butyldimethylsilanyloxy)ethyl]-2-hydroxyphenyl}formamide | HCID 57461065 | — |
Reaction Steps
The title compound was synthesized in a manner analogous to that described for Intermediate 2, using Intermediate 12 in place of Intermediate 1. ES/MS calcd. C15H27N2O3Si+ 311.2. Found m/z=311 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394829B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-f57d61e0339a4bff83b4a471abd55596 |
| Source note | uspto-grants-2013_03 |