4-Iodo-o-toluidine → HCID 723685, compound

HRID 1944866Notes

Reaction equation

HRID 1944866 reaction equation
[F:1][C:2]([F:14])([F:13])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([I:12])=[CH:8][CH:7]=1)=[O:4].I[C:16]1C=CC(N)=C(C)C=1>>[F:14][C:2]([F:1])([F:13])[C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([I:12])=[CH:8][C:7]=1[CH3:16])=[O:4]

Participants

3

Reactant 2

HCID 832214-Iodo-o-toluidineHCID 6869622,2,2-trifluoro-N-(4-iodophenyl)acetamide

Product 1

HCID 723685HCID 723685, compound

Procedure

Title compound was synthesized in a manner analogous to Intermediate 32 using 4-iodo-2-methylaniline as a substrate. ES/MS calcd. for C9H7F3INO 328.95. Found m/z=330 (M+H)+.

Sources & evidence

ORD record
ord-f1792115b34b4ffeb39d11fbda25c050
Source dataset
uspto-grants-2013_03
Patent number
US08394829B2

Reaction notes

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