1-Iodo-3-nitrobenzene → HCID 57516942, compound

HRID 1944875Notes

Reaction equation

HRID 1944875 reaction equation
FC(F)(F)C(NC1C=CC(C#[C:13][CH2:14][CH2:15][CH2:16][CH2:17][OH:18])=CC=1)=O.I[C:22]1[CH:23]=[C:24]([N+:28]([O-:30])=[O:29])[CH:25]=[CH:26][CH:27]=1>>[N+:28]([C:24]1[CH:23]=[C:22]([C:13]#[C:14][CH2:15][CH2:16][CH2:17][OH:18])[CH:27]=[CH:26][CH:25]=1)([O-:30])=[O:29]

Participants

3

Reactant 2

HCID 125741-Iodo-3-nitrobenzeneHCID 575169382,2,2-trifluoro-N-(4-(6-hydroxyhex-1-yn-1-yl)phenyl)acetamide

Product 1

HCID 57516942HCID 57516942, compound

Procedure

The title compound was synthesized in a manner analogous to that described for Intermediate 39, using 3-iodonitrobenzene as a substrate. ES/MS calcd. for C11H12NO3+ 206.1. Found m/z=206.2 (M+H)+.

Sources & evidence

ORD record
ord-49f01867e9924fd1b8678f2a3760a1d0
Source dataset
uspto-grants-2013_03
Patent number
US08394829B2

Reaction notes

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