HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(4-chloro-2-methoxyphenoxy)acetate → (4-Chloro-2-hydroxyphenoxy)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(4-chloro-2-methoxyphenoxy)acetate | HCID 11701508 | — |
| Solvent | Hydrogen Bromide | HCID 260 | — |
| Product | (4-Chloro-2-hydroxyphenoxy)acetic acid | HCID 16748825 | — |
Reaction Steps
A mixture of the product from step (i) (2.7 g) in 48% aqueous hydrogen bromide (30 ml) was heated under reflux for 2 h. The solvent was evaporated, the residue washed with water and dried, yield 1.7 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-2f33f75fc6134b3bbe73b114e5929d8d |
| Source note | uspto-grants-2013_03 |