HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 243441, compound → 6-Chloro-2H-1,4-benzoxazin-3(4H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 243441 | HCID 243441 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 6-Chloro-2H-1,4-benzoxazin-3(4H)-one | HCID 309259 | — |
Reaction Steps
Iron powder (1.4 g) was added to a solution of the product from step (i) (1.4 g) in acetic acid (30 ml) and the mixture stirred at RT for 1 h. The mixture was filtered and the filtrate evaporated under reduced pressure. Yield 0.44 g
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394986B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-145db10e0553491ea65a4b4cd7994a74 |
| Source note | uspto-grants-2013_03 |