Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nonan-5-ol | HCID 12202 | — |
| Reactant | Sodium 2-Iodobenzenesulfonate | HCID 23662047 | — |
| Reactant | Potassium hydroxy sulfite | HCID 23707502 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 5-Nonanone | HCID 10405 | — |
Reaction Steps
9.2 mg (0.03 mmol) of sodium 2-iodobenzenesulfonate prepared by Preparation Example 4, 1.48 g (2.4 mmol) of Oxone (registered trademark) and 433 mg (3 mmol) of 5-nonanol were added to 3.75 ml of acetonitrile, and the mixture was heated at 70° C. while being stirred for three hours. The later treatment was carried out in the same way as in Example 1, and then 5-nonanone was obtained. The yield of the obtained 5-nonanone was determined and the result is shown in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08394995B2 |
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| Source dataset | uspto-grants-2013_03 |
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| ORD ID | ord-9cc0acf0635546158759a34d09784575 |
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| Source note | uspto-grants-2013_03 |
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