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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1945249Generated: October 30, 2026

Nonan-5-ol → 5-Nonanone

https://huagongshe.com/reaction/1945249

Reaction equation

Participants

RoleNameHCIDCharge
ReactantNonan-5-olHCID 12202—
ReactantSodium 2-IodobenzenesulfonateHCID 23662047—
ReactantPotassium hydroxy sulfiteHCID 23707502—
SolventAcetonitrileHCID 6342—
Product5-NonanoneHCID 10405—

Reaction Conditions

Temperature70 °C

Reaction Steps

9.2 mg (0.03 mmol) of sodium 2-iodobenzenesulfonate prepared by Preparation Example 4, 1.48 g (2.4 mmol) of Oxone (registered trademark) and 433 mg (3 mmol) of 5-nonanol were added to 3.75 ml of acetonitrile, and the mixture was heated at 70° C. while being stirred for three hours. The later treatment was carried out in the same way as in Example 1, and then 5-nonanone was obtained. The yield of the obtained 5-nonanone was determined and the result is shown in Table 1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08394995B2
Source datasetuspto-grants-2013_03
ORD IDord-9cc0acf0635546158759a34d09784575
Source noteuspto-grants-2013_03