HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzimidazole → HCID 59606080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzimidazole | HCID 11984 | — |
| Reactant | HCID 87420997 | HCID 87420997 | — |
| Product | HCID 59606080 | HCID 59606080 | — |
Reaction Steps
Following General Procedure I for Buchwald coupling, 2-methylbenzimidazole and racemic 2-(4-((2-chloro-9-methyl-6-morpholino-9H-purin-8-yl)methyl)piperazin-1-yl)-3-methylbutan-1-ol were reacted. The enantiomers were separated by SFC to give 361. LCMS m/z: 534.3 (MH+)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08394796B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-96de5ddaad04481e9fcd99ceda600779 |
| Source note | uspto-grants-2013_03 |