HRID1946258

反应详情

EQUATION

反应方程式

HRID 1946258 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1-(3,4-dinitrobenzyl)-4-methylpiperazine (1 g) was dissolved in DMF:MeOH (1:1, 20 mil) and agitated with 10% Pd/C (50 mg) under an atmosphere of H2 for 6 hours. The mixture was then filtered and evaporated to give a dark solid which was used immediately without any further purification.

WORKUP

后处理

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  2. customevaporated
  3. customto give a dark solid which
  4. customwas used immediately without any further purification