Ethyl Acetate → HCID 58460230, compound

Participants

Reaction Conditions

Reaction Steps

Ethyl acetate (0.234 mL) in dry THF (1 ml) was added dropwise to a stirred solution of LiHMDS, 1M in THF (2.389 mL) cooled to −78° C. under nitrogen atmosphere. The mixture was stirred at −78° C. for 30 minutes. Then, Intermediate 18 (230 mg) in THF (2 ml) was added dropwise. The RM was stirred at −78° C. under nitrogen for 1 hour.

Provenance & Evidence