HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-3-methylbenzene-1-sulfonamide → HCID 25182773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-3-methylbenzene-1-sulfonamide | HCID 143037 | — |
| Reactant | 6-[Cyclohexyl(cyclopropylmethyl)amino]pyrimidine-4-carboxylic acid | HCID 59446841 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 25182773 | HCID 25182773 | — |
Reaction Steps
Following the general method as outlined in Example 1, starting from 6-[cyclohexyl(cyclopropylmethyl)amino]pyrimidine-4-carboxylic acid (Intermediate 13) and 4-amino-3-methyl-benzenesulfonamide (Biofine), the title compound was obtained as an off-white solid after trituration in methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399448B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-72a39c1ecaba4df1957c986074a2a83a |
| Source note | uspto-grants-2013_03 |