HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzamide → HCID 25182778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzamide | HCID 76079 | — |
| Reactant | 6-[Cyclohexyl(cyclopropylmethyl)amino]pyrimidine-4-carboxylic acid | HCID 59446841 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 25182778 | HCID 25182778 | 85% |
Reaction Steps
Following the general method as outlined in Example 1, starting from 6-[cyclohexyl(cyclopropylmethyl)amino]pyrimidine-4-carboxylic acid (Intermediate 13) and 4-aminobenzamide (Aldrich), the title compound was obtained as a brown solid in 85% yield after trituration in DCM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08399448B2 |
| Source dataset | uspto-grants-2013_03 |
| ORD ID | ord-b8f89070b1514a9b9a69264eb3051d19 |
| Source note | uspto-grants-2013_03 |